S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Base Information

Chemical Name:S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate
CAS No.:1170733-41-1
Molecular Formula:C₂₀H₂₁F₃N₂O₅S
Molecular Weight:458.458
Hs Code.:

Synonyms:S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

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Chemical Property of S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

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Technology Process of S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

There total 5 articles about S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.1%

: 1170733-40-0
S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

: 1170733-41-1
S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Guidance literature:: With silver nitrate; In acetonitrile; for 6h; Reflux; Inert atmosphere; Darkness;
DOI:10.1021/ml2000033

Reference yield:

: C₁₈H₁₇ClF₃NO₂

: 1170733-41-1
S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 8 h / 25 °C / Inert atmosphere

2.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 0 - 25 °C / Inert atmosphere

3.1: silver nitrate / acetonitrile / 6 h / Reflux; Inert atmosphere; Darkness

With silver nitrate; triethylamine; triphenylphosphine; In dichloromethane; acetonitrile;
DOI:10.1021/ml2000033

Reference yield:

: C₂₁H₂₀F₃N₃O₂

: 1170733-41-1
S-2-(nitrooxy)ethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 12 h / 25 °C / Inert atmosphere

2.1: triethylamine / acetonitrile / 24 h / 0 - 25 °C / Inert atmosphere

3.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

3.2: 0 - 25 °C / Inert atmosphere

4.1: silver nitrate / acetonitrile / 6 h / Reflux; Inert atmosphere; Darkness

With silver nitrate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ml2000033