6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene

Base Information

• Chemical Name: 6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene
• CAS No.: 101893-03-2
• Molecular Formula: C₁₈H₂₈
• Molecular Weight: 244.42
• Mol file: 101893-03-2.mol

Synonyms:6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene

Chemical Property of 6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene

There total 2 articles about 6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butylbenzene (253185-03-4,253185-04-5) + 2,5-dichloro-2,5-dimethyl hexane (6223-78-5) → 1,4-di-tert-butylbenzene (1012-72-2) + 1,1,4,4,5,5,8,8-octamethyl-1,2,3,4,5,6,7,8-octahydroanthracene (22306-30-5) + 6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene (101893-03-2)

Guidance literature:

With aluminium trichloride; In pentane; for 0.666667h; Ambient temperature;

DOI:10.1021/jo01075a008

Reference yield:

1,4-di-tert-butylbenzene (1012-72-2) + tertiary butyl chloride (507-20-0) → 1,3,5-Tri-tert-butylbenzene (1460-02-2) + 1,3-di-tert-butylbenzene (1014-60-4) + 1,1,4,4,5,5,8,8-octamethyl-1,2,3,4,5,6,7,8-octahydroanthracene (22306-30-5) + 6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene (101893-03-2)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; at -5 - 5 ℃;

DOI:10.1021/jo01075a008

Reference yield:

6-tert-butyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydro-naphthalene (101893-03-2) + acetyl chloride (75-36-5) → 1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphth-2-yl)ethanone (17610-21-8)

Guidance literature:

With aluminium trichloride; 1,2-dichloro-ethane;

upstream raw materials:

tert-butylbenzene

2,5-dichloro-2,5-dimethyl hexane

1,4-di-tert-butylbenzene

tertiary butyl chloride

Downstream raw materials:

1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphth-2-yl)ethanone