C₃₉H₅₀O₆

Base Information

Chemical Name:C₃₉H₅₀O₆
CAS No.:211695-04-4
Molecular Formula:C₃₉H₅₀O₆
Molecular Weight:614.822
Hs Code.:

C<sub>39</sub>H<sub>50</sub>O<sub>6</sub>

Synonyms:C₃₉H₅₀O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₅₀O₆

Chemical Property:

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Technology Process of C₃₉H₅₀O₆

There total 20 articles about C₃₉H₅₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 98-88-4
benzoyl chloride

: (5E,10E,14E)-(1S,2R,3S,3aR,7S,16aS)-3-((S)-2-Hydroxy-1-methyl-ethyl)-6,10,14,16a-tetramethyl-1,2,3,3a,4,7,8,9,12,13,16,16a-dodecahydro-cyclopentacyclopentadecene-1,2,7-triol

: 211695-04-4
C₃₉H₅₀O₆

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 5h;
DOI:10.7164/antibiotics.51.602

Reference yield:

: 201685-07-6
Acetic acid (4E,8E)-10-chloro-1-[1-(diethoxy-phosphoryl)-ethyl]-4,8-dimethyl-deca-4,8-dienyl ester

: 211695-04-4
C₃₉H₅₀O₆

Guidance literature:: Multi-step reaction with 18 steps

1: 90 percent / Cs₂CO₃; CsI / acetonitrile / 3 h / 50 °C

2: NaBH₄ / methanol / 0.25 h / 0 °C

3: 92 percent / DIPEA / 1,2-dichloro-ethane / 1 h / 60 °C

4: LiOH / H₂O; methanol / 1 h / 60 °C

5: 80 percent / hexamethylphosphoric acid triamide / 0.5 h / 20 °C

6: 78 percent / TPAP; NMO / CH₂Cl₂ / 3 h / 20 °C

7: 75 percent / DIPEA; LiCl / acetonitrile / 72 h / 20 °C

8: Li-n-BuBH₃ / tetrahydrofuran / 0.5 h / 20 °C

9: 78 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

10: 88 percent / LiAlH₄ / diethyl ether / 0.25 h / 0 °C

11: PDC / zeolite / CH₂Cl₂ / 2 h / 20 °C

12: 65 percent / NH₂NH₂*H₂O; NaOH / triethylene glycol / 2 h / 190 °C

13: TBAF / tetrahydrofuran / 12 h / 60 °C

14: 92 percent / MnO₂ / CH₂Cl₂ / 48 h / 20 °C

15: 90 percent / (S)-BINAL-H / CH₂Cl₂; tetrahydrofuran / 1 h / -10 °C

16: 2M HCl / tetrahydrofuran / 3 h / 60 °C

17: NaBH₄ / methanol / 15 h / 20 °C

18: 62 percent / pyridine; DMAP / CH₂Cl₂ / 5 h / 20 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; dmap; manganese(IV) oxide; lithium hydroxide; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; dipyridinium dichromate; isocyanate de chlorosulfonyle; N-methyl-2-indolinone; tetrapropylammonium perruthennate; (-)-(S)-BINAL-H; Li-n-BuBH₃; tetrabutyl ammonium fluoride; caesium carbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; lithium chloride; zeolite; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; 1: Alkylation / 2: Reduction / 3: Alkylation / 4: Ring cleavage / 5: Esterification / 6: Oxidation / 7: Cyclization / 8: Reduction / 9: Substitution / 10: Reduction / 11: Oxidation / 12: Reduction / 13: Hydrolysis / 14: Oxidation / 15: Reduction / 16: Hydrolysis / 17: Ring cleavage / 18: Acylation;
DOI:10.7164/antibiotics.51.602

Reference yield:

: (2S,3S,3aS,3bR,8aR)-2-Benzyloxy-3-methyl-octahydro-furo[3',2':3,4]cyclopenta[1,2-c]pyran-7,8-dione

: 211695-04-4
C₃₉H₅₀O₆

Guidance literature:: Multi-step reaction with 18 steps

1: 90 percent / Cs₂CO₃; CsI / acetonitrile / 3 h / 50 °C

2: NaBH₄ / methanol / 0.25 h / 0 °C

3: 92 percent / DIPEA / 1,2-dichloro-ethane / 1 h / 60 °C

4: LiOH / H₂O; methanol / 1 h / 60 °C

5: 80 percent / hexamethylphosphoric acid triamide / 0.5 h / 20 °C

6: 78 percent / TPAP; NMO / CH₂Cl₂ / 3 h / 20 °C

7: 75 percent / DIPEA; LiCl / acetonitrile / 72 h / 20 °C

8: Li-n-BuBH₃ / tetrahydrofuran / 0.5 h / 20 °C

9: 78 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

10: 88 percent / LiAlH₄ / diethyl ether / 0.25 h / 0 °C

11: PDC / zeolite / CH₂Cl₂ / 2 h / 20 °C

12: 65 percent / NH₂NH₂*H₂O; NaOH / triethylene glycol / 2 h / 190 °C

13: TBAF / tetrahydrofuran / 12 h / 60 °C

14: 92 percent / MnO₂ / CH₂Cl₂ / 48 h / 20 °C

15: 90 percent / (S)-BINAL-H / CH₂Cl₂; tetrahydrofuran / 1 h / -10 °C

16: 2M HCl / tetrahydrofuran / 3 h / 60 °C

17: NaBH₄ / methanol / 15 h / 20 °C

18: 62 percent / pyridine; DMAP / CH₂Cl₂ / 5 h / 20 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; dmap; manganese(IV) oxide; lithium hydroxide; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; dipyridinium dichromate; isocyanate de chlorosulfonyle; N-methyl-2-indolinone; tetrapropylammonium perruthennate; (-)-(S)-BINAL-H; Li-n-BuBH₃; tetrabutyl ammonium fluoride; caesium carbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; lithium chloride; zeolite; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; 1: Alkylation / 2: Reduction / 3: Alkylation / 4: Ring cleavage / 5: Esterification / 6: Oxidation / 7: Cyclization / 8: Reduction / 9: Substitution / 10: Reduction / 11: Oxidation / 12: Reduction / 13: Hydrolysis / 14: Oxidation / 15: Reduction / 16: Hydrolysis / 17: Ring cleavage / 18: Acylation;
DOI:10.7164/antibiotics.51.602