(E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

Base Information

Chemical Name:(E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate
CAS No.:1316832-71-9
Molecular Formula:C₄₆H₄₇N₈O₁₄P
Molecular Weight:966.898
Hs Code.:

(E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

Synonyms:(E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

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Chemical Property of (E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

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Technology Process of (E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

There total 11 articles about (E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₁₈H₂₃N₅O

: 1316832-66-2
C₃₄H₂₉N₄O₁₆P

: 1316832-71-9
(E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ja200808y

Reference yield:

: 1316832-58-2
allyl 2-(2-hydroxy-2-(4-hydroxyphenyl)acetamido)acetate

: 1316832-71-9
(E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / dichloromethane / 0.17 h / 20 °C

1.2: 6 h / 20 °C / Cooling with ice

2.1: dmap / dichloromethane / 0.17 h / Cooling with ice

2.2: 7 h / 20 °C / Cooling with ice

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C

With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja200808y

Reference yield:

: 1316832-63-9
allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

: 1316832-71-9
(E)-allyl 9-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-1-(4-((4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10-trioxo-8-oxa-2,6,11-triazatridecan-13-oate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap / dichloromethane / 0.17 h / Cooling with ice

1.2: 7 h / 20 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C

With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja200808y