allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

Base Information

Chemical Name:allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate
CAS No.:1316832-63-9
Molecular Formula:C₂₇H₂₆N₃O₁₂P
Molecular Weight:615.49
Hs Code.:

Synonyms:allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

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Chemical Property of allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

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Technology Process of allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

There total 5 articles about allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1316832-58-2
allyl 2-(2-hydroxy-2-(4-hydroxyphenyl)acetamido)acetate

: 56883-17-1
di(2-nitrobenzyl) chlorophosphate

: 1316832-63-9
allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

Guidance literature:: allyl 2-(2-hydroxy-2-(4-hydroxyphenyl)acetamido)acetate; With dmap; In dichloromethane; at 20 ℃; for 0.166667h;

di(2-nitrobenzyl) chlorophosphate; With triethylamine; In dichloromethane; at 20 ℃; for 6h; Cooling with ice;
DOI:10.1021/ja200808y

Reference yield:

: 59765-55-8
glycine allyl ester

: 1316832-63-9
allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.17 h / Cooling with ice

1.2: 20 °C / Cooling with ice

2.1: dmap / dichloromethane / 0.17 h / 20 °C

2.2: 6 h / 20 °C / Cooling with ice

With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja200808y

Reference yield:

: 612-25-9
2-Nitrobenzyl alcohol

: 1316832-63-9
allyl 2-(2-(4-(bis(2-nitrobenzyloxy)phosphoryloxy)phenyl)-2-hydroxyacetamido)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; phosphorodichloridic acid

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

3.1: dmap / dichloromethane / 0.17 h / 20 °C

3.2: 6 h / 20 °C / Cooling with ice

With pyridine; dmap; oxalyl dichloride; phosphorodichloridic acid; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ja200808y