(1R,2R,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid

Base Information

• Chemical Name: (1R,2R,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid
• CAS No.: 141042-73-1
• Molecular Formula: C₁₅H₁₇NO₄
• Molecular Weight: 275.304

Synonyms:(1R,2R,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid

Chemical Property of (1R,2R,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid

Chemical Property:

Purity/Quality:

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Technology Process of (1R,2R,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid

There total 14 articles about (1R,2R,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-(4-morpholinylcarbonyl)-2-formyl-3-phenylcyclopropane (140926-05-2,141042-62-8,141506-51-6,141506-55-0,141506-57-2,141506-58-3) → (1S,2S,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid (130780-73-3,130855-62-8,141042-66-2,141042-69-5,141042-73-1,141042-77-5,141506-33-4,141506-36-7)

Guidance literature:

With jones reagent; In acetone; at 0 ℃; for 2h;

DOI:10.1016/S0040-4039(00)97718-9

Reference yield:

((1R,2R,3S)-2-Hydroxymethyl-3-phenyl-cyclopropyl)-morpholin-4-yl-methanone (130780-69-7,141041-95-4,141506-48-1,141506-56-1) → (1R,2R,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid (141042-73-1)

Guidance literature:

With jones' reagent; In ethanol; acetone; at 0 - 5 ℃; for 2h;

DOI:10.1021/jm00088a005

Reference yield:

((1S,2S,3R)-2-Hydroxymethyl-3-phenyl-cyclopropyl)-morpholin-4-yl-methanone (130780-69-7,141041-95-4,141506-48-1,141506-56-1) → (1S,2S,3S)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid (130780-73-3,130855-62-8,141042-66-2,141042-69-5,141042-73-1,141042-77-5,141506-33-4,141506-36-7)

Guidance literature:

With jones reagent; In acetone; at 0 ℃; for 2h; Yield given;

DOI:10.1016/S0040-4039(00)97718-9

upstream raw materials:

((1S,2S,3R)-2-Hydroxymethyl-3-phenyl-cyclopropyl)-morpholin-4-yl-methanone

(Z)-cinnamyl alcohol

endo-6-phenyl-3-oxabicyclo<3.1.0>hexan-2-one

cis-3-phenyl-2-propen-1-yl diazoacetate

Downstream raw materials:

(1R,2R,3S)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid [(S)-1-((1S,2R,3S)-1-cyclohexylmethyl-2,3-dihydroxy-5-methyl-hexylcarbamoyl)-2-thiazol-4-yl-ethyl]-amide

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