Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester

Base Information

Chemical Name:Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester
CAS No.:203261-33-0
Molecular Formula:C₄₀H₄₄O₆
Molecular Weight:620.786
Hs Code.:

Synonyms:Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester

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Chemical Property of Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester

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Technology Process of Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester

There total 4 articles about Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 83526-68-5
(S)-1-(benzyloxy)-3-trityloxypropan-2-ol

: suberic acid monoallyl ester

: 203261-33-0
Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide;
DOI:10.1021/ja971270t

Reference yield:

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 203261-33-0
Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Et₃N, DMAP

2: 97 percent / DCC, DMAP

With dmap; triethylamine; dicyclohexyl-carbodiimide;
DOI:10.1021/ja971270t

Reference yield:

: 100-39-0
benzyl bromide

: 203261-33-0
Octanedioic acid allyl ester (S)-1-benzyloxymethyl-2-trityloxy-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaH

2: 1N aq. HCl

3: 94 percent / Et₃N, DMAP

4: 97 percent / DCC, DMAP

With hydrogenchloride; dmap; sodium hydride; triethylamine; dicyclohexyl-carbodiimide;
DOI:10.1021/ja971270t