1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Base Information

• Chemical Name: 1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene
• CAS No.: 1381848-03-8
• Molecular Formula: C₅₃H₆₂N₄O₅
• Molecular Weight: 835.099

Synonyms:1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Chemical Property of 1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Chemical Property:

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Technology Process of 1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

There total 3 articles about 1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene (1381848-01-6) → 1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene (1381848-03-8)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c2cc31512b

Reference yield:

1,3,5-Triethynylbenzene (7567-63-7) → 1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene (1381848-03-8)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 23 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 13 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid / 1 h / 20 °C / Inert atmosphere

With triethylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1039/c2cc31512b

Reference yield:

4-(tert-butoxycarbonylamino)benzohydroximinoyl chloride (190446-52-7) → 1-[3-(4-aminophenyl)isoxazol-5-yl]-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene (1381848-03-8)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 23 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 13 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid / 1 h / 20 °C / Inert atmosphere

With triethylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1039/c2cc31512b

upstream raw materials:

1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

1,3,5-Triethynylbenzene

4-(tert-butoxycarbonylamino)benzohydroximinoyl chloride

Downstream raw materials:

N-{4-{5-{3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}phenyl}isoxazol-3-yl}phenyl}-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

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