1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Base Information

Chemical Name:1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene
CAS No.:1381848-01-6
Molecular Formula:C₅₈H₇₀N₄O₇
Molecular Weight:935.216
Hs Code.:

Synonyms:1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

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Chemical Property of 1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

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Technology Process of 1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

There total 3 articles about 1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: C₁₇H₂₇ClN₂O

: 1381847-97-7
1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-diethynylbenzene

: 1381848-01-6
1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 13h; Inert atmosphere;
DOI:10.1039/c2cc31512b

Reference yield:

: 7567-63-7
1,3,5-Triethynylbenzene

: 1381848-01-6
1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 23 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 13 h / 20 °C / Inert atmosphere

With triethylamine; In dichloromethane;
DOI:10.1039/c2cc31512b

Reference yield:

: 190446-52-7
4-(tert-butoxycarbonylamino)benzohydroximinoyl chloride

: 1381848-01-6
1-{3-[4-(N-tert-butoxycarbonyl)aminophenyl]isoxazol-5-yl}-3,5-bis{3-[(S)-(+)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 23 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 13 h / 20 °C / Inert atmosphere

With triethylamine; In dichloromethane;
DOI:10.1039/c2cc31512b