C₂₈H₂₆FNO₇S

Base Information

Chemical Name:C₂₈H₂₆FNO₇S
CAS No.:1374233-82-5
Molecular Formula:C₂₈H₂₆FNO₇S
Molecular Weight:539.581
Hs Code.:

C<sub>28</sub>H<sub>26</sub>FNO<sub>7</sub>S

Synonyms:C₂₈H₂₆FNO₇S

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Chemical Property of C₂₈H₂₆FNO₇S

Chemical Property:

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Technology Process of C₂₈H₂₆FNO₇S

There total 12 articles about C₂₈H₂₆FNO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1374233-81-4
C₂₆H₂₄FNO₇S

: 247129-85-7
(2-bromoethyl)(diphenyl)sulfonium trifluoromethanesulfonate

: 1374233-82-5
C₂₈H₂₆FNO₇S

Guidance literature:: With sodium hydride; In dichloromethane; paraoil; at 0 - 20 ℃; for 15h;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374233-82-5
C₂₈H₂₆FNO₇S

Guidance literature:: Multi-step reaction with 12 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: boron trichloride / dichloromethane / -78 - -40 °C

6.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

7.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

8.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

9.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

9.2: 20 °C / pH 8 - 9

10.1: pyridine / 2 h / 0 - 30 °C

11.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / 0 °C

12.1: sodium hydride / dichloromethane; paraoil / 15 h / 0 - 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; potassium phosphate; tin(II) chloride dihdyrate; water; nitric acid; sodium acetate; boron trichloride; sodium hydride; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; paraoil; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374233-82-5
C₂₈H₂₆FNO₇S

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: boron trichloride / dichloromethane / -78 - -40 °C

7.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

8.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

9.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

10.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

10.2: 20 °C / pH 8 - 9

11.1: pyridine / 2 h / 0 - 30 °C

12.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / 0 °C

13.1: sodium hydride / dichloromethane; paraoil / 15 h / 0 - 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; potassium phosphate; tin(II) chloride dihdyrate; water; nitric acid; sodium acetate; boron trichloride; sodium hydride; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; paraoil; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;