(2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane

Base Information

Chemical Name:(2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane
CAS No.:1263293-11-3
Molecular Formula:C₄₉H₇₈O₈Si₂
Molecular Weight:851.325
Hs Code.:

Synonyms:(2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane

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Chemical Property of (2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane

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Technology Process of (2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane

There total 1 articles about (2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1263293-04-4
(2R,4R,8R,10R)-1-(benzyloxy)-12-((tert-butyl)dimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecan-4-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1263293-11-3
(2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 25 ℃;
DOI:10.1002/chem.201002204

Reference yield: 91.0%

: 1263293-11-3
(2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane

: 1263293-09-9
(2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis((tert-butyl)dimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecan-6-one

Guidance literature:: (2R,4R,8R,10R)-1-(benzyloxy)-4,12-bis(tert-butyldimethylsilyloxy)-8-methoxy-2,10-bis(4-methoxybenzyloxy)-6-methylenedodecane; With ozone; In dichloromethane; at -78 ℃; for 0.0833333h;

With oxygen; In dichloromethane; at -78 ℃; for 0.166667h;

With dimethylsulfide; In dichloromethane; at -78 - 25 ℃;
DOI:10.1002/chem.201002204