1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

Base Information

Chemical Name:1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose
CAS No.:937181-57-2
Molecular Formula:C₁₇H₁₆F₂O₇
Molecular Weight:370.307
Hs Code.:

Synonyms:1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

Suppliers and Price of 1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

There total 3 articles about 1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 937181-56-1
5-O-benzoyl-3-deoxy-1,2-O-isopropylidene-3,4-C-(difluoromethylene)-β-L-arabinofuranose

: 108-24-7
acetic anhydride

: 937181-57-2
1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

Guidance literature:: With sulfuric acid; acetic acid; at 20 ℃; for 8h;
DOI:10.1021/jo062614d

Reference yield:

: 94795-73-0
5-O-benzoyl-1,2-O-isopropylidene-3-deoxy-α-D-glycero-pent-3-enofuranose

: 937181-57-2
1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / NaI / tetrahydrofuran / 2 h / 70 °C

2: 55 percent / acetic acid; conc. H₂SO₄ / 8 h / 20 °C

With sulfuric acid; acetic acid; sodium iodide; In tetrahydrofuran;
DOI:10.1021/jo062614d

Reference yield:

: 94795-72-9
1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-xylofuranose

: 937181-57-2
1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3,4-C-(difluoromethylene)-L-arabinofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / DBU / toluene / 1 h / 80 °C

2: 99 percent / NaI / tetrahydrofuran / 2 h / 70 °C

3: 55 percent / acetic acid; conc. H₂SO₄ / 8 h / 20 °C

With sulfuric acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In tetrahydrofuran; toluene;
DOI:10.1021/jo062614d