Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate

Base Information

• Chemical Name: Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate
• CAS No.: 73591-44-3
• Molecular Formula: C₁₃H₁₂N₆O₈
• Molecular Weight: 380.274

Synonyms:Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate

Chemical Property of Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate

There total 3 articles about Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Dimethyl 1,3-Acetonedicarboxylate (2,4-Dinitrophenyl)hydrazone (73591-43-2) → Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate (73591-44-3)

Guidance literature:

With 4-toluenesulfonyl azide; 1,5-Diazabicyclo[5.4.0]undec-5-ene; In ethyl acetate; for 1h; Ambient temperature;

DOI:10.1002/jhet.5570170132

Reference yield:

3-oxopentanedioic acid dimethyl ester (1830-54-2) → Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate (73591-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 88.9 percent / conc. sulfuric acid / H₂O; methanol / 2 h

2: 90 percent / p-toluenesulfonyl azide, 1,5-diazabicyclo<5.4.0>undec-5-ene / ethyl acetate / 1 h / Ambient temperature

With 4-toluenesulfonyl azide; sulfuric acid; 1,5-Diazabicyclo[5.4.0]undec-5-ene; In methanol; water; ethyl acetate;

DOI:10.1002/jhet.5570170132

Reference yield:

(2,4-dinitro-phenyl)-hydrazine (119-26-6) → Methyl 5-Methoxycarbonylmethyl-1-(2,4-dinitroanilino)-1,2,3-triazole-4-carboxylate (73591-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 88.9 percent / conc. sulfuric acid / H₂O; methanol / 2 h

2: 90 percent / p-toluenesulfonyl azide, 1,5-diazabicyclo<5.4.0>undec-5-ene / ethyl acetate / 1 h / Ambient temperature

With 4-toluenesulfonyl azide; sulfuric acid; 1,5-Diazabicyclo[5.4.0]undec-5-ene; In methanol; water; ethyl acetate;

DOI:10.1002/jhet.5570170132

upstream raw materials:

Dimethyl 1,3-Acetonedicarboxylate (2,4-Dinitrophenyl)hydrazone

3-oxopentanedioic acid dimethyl ester

(2,4-dinitro-phenyl)-hydrazine

Downstream raw materials:

Methyl 5-Cyanomethyl-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,3-triazole-4-carboxylate

Methyl 4-Cyanomethyl-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,3-triazole-5-carboxylate

Methyl 5-Cyanomethyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,3-triazole-4-carboxylate

5-Cyanomethyl-2-(β-D-ribofuranosyl)-1,2,3-triazole-4-carboxamide

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