Technology Process of C36H46N4O18
There total 5 articles about C36H46N4O18 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C16H19N3O6; C24H38NO16P;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Molecular sieve;
Inert atmosphere;
With
trimethylsilyl trifluoromethanesulfonate;
In
tetrahydrofuran;
Molecular sieve;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: boron trifluoride diethyl etherate / dichloromethane / 6 h / Reflux
2.1: sodium methylate; methanol / 0.5 h / 20 °C
3.1: camphor-10-sulfonic acid / acetonitrile / 18 h / 20 °C
4.1: pyridine; dmap / 24 h / 20 °C / Cooling with ice
5.1: strongly acidic resin / methanol / 4 h / 40 °C
6.1: tetrahydrofuran / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere
6.2: Molecular sieve; Inert atmosphere
With
pyridine; methanol; dmap; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium methylate; methanol / 0.5 h / 20 °C
2.1: camphor-10-sulfonic acid / acetonitrile / 18 h / 20 °C
3.1: pyridine; dmap / 24 h / 20 °C / Cooling with ice
4.1: strongly acidic resin / methanol / 4 h / 40 °C
5.1: tetrahydrofuran / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere
5.2: Molecular sieve; Inert atmosphere
With
pyridine; methanol; dmap; camphor-10-sulfonic acid; sodium methylate;
In
tetrahydrofuran; methanol; acetonitrile;
