1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

Base Information

Chemical Name:1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose
CAS No.:84278-00-2
Molecular Formula:C14H19 N3 O9
Molecular Weight:373.32
Hs Code.:
European Community (EC) Number:633-035-0
DSSTox Substance ID:DTXSID10447866
Nikkaji Number:J774.536B
Mol file:84278-00-2.mol

Synonyms:84278-00-2;1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose;[(2R,3R,4R,5R)-3,4,6-triacetyloxy-5-azidooxan-2-yl]methyl acetate;2-AZIDO-2-DEOXY-1,3,4,6-TETRA-O-ACETYL-ALPHA/BETA-D-GALACTOPYRANOSE;2-Azido-D-galactose tetraacetate;2-Azido-2-deoxy-D-galactose tetraacetate;SCHEMBL18857676;DTXSID10447866;QKGHBQJLEHAMKJ-RQICVUQASA-N;MFCD02683262;AKOS025295799;2-Azido-2-deoxy-D-galactopyranose tetraacetate;2-Azido-D-galactose tetraacetate, >=97% (HPLC);W-203910;2-azido-2-deoxy-1,3,4,6-tetra-O-acetyl-alpha,beta-D-galactopyranose

Suppliers and Price of 1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Azido-2-deoxy-1,3,4,6-tetra-O-acetyl-D-galactopyranose
100mg
$ 60.00

TRC
2-Azido-2-deoxy-1,3,4,6-tetra-O-acetyl-D-galactopyranose
1g
$ 260.00

Sigma-Aldrich
2-Azido-D-galactose tetraacetate ≥97% (HPLC)
250mg
$ 215.00

Medical Isotopes, Inc.
1-3-4-6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose
500 mg
$ 595.00

Iris Biotech GmbH
D-Gal(N3, Ac3)-OAc
1 g
$ 715.50

Iris Biotech GmbH
D-Gal(N3, Ac3)-OAc
2 g
$ 1107.00

Iris Biotech GmbH
D-Gal(N3, Ac3)-OAc
250 mg
$ 297.00

Biosynth Carbosynth
1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose
250 mg
$ 125.00

Biosynth Carbosynth
1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose
100 mg
$ 75.00

Biosynth Carbosynth
1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose
500 mg
$ 195.00

Total 15 raw suppliers

Chemical Property of 1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

Chemical Property:

Melting Point:113-114°C
PSA：164.18000
LogP:-0.16744
Storage Temp.:Hygroscopic, Refrigerator, Under Inert Atmosphere
XLogP3:0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:11
Rotatable Bond Count:10
Exact Mass:373.11212919
Heavy Atom Count:26
Complexity:617

Purity/Quality:

99%, ^*data from raw suppliers

2-Azido-2-deoxy-1,3,4,6-tetra-O-acetyl-D-galactopyranose ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 20/21/22-36/37/38-68
Safety Statements: 26-36/37

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OCC1C(C(C(C(O1)OC(=O)C)N=[N+]=[N-])OC(=O)C)OC(=O)C
Isomeric SMILES:CC(=O)OC[C@@H]1[C@@H]([C@@H]([C@H](C(O1)OC(=O)C)N=[N+]=[N-])OC(=O)C)OC(=O)C

Technology Process of 1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

There total 13 articles about 1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-24-7
acetic anhydride

: 3,4,6-tri-O-acetyl-2-azido-2-deoxy-D-galactopyranose

: 84278-00-2
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

Guidance literature:: With pyridine; at 20 ℃; for 15h;
DOI:10.1016/j.carres.2008.11.018

Reference yield: 95.0%

: 127-09-3
sodium acetate

: 3,4,6-tri-O-acetyl-2-azido-2-deoxy-D-galactopyranosyl nitrate

: 84278-00-2
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

Guidance literature:: In acetic acid; at 120 ℃; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jacs.9b06830

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 1772-03-8,4710-95-6,6730-09-2,14131-59-0,14131-62-5,14131-63-6,14131-65-8,14131-67-0,14257-79-5,19124-46-0,20706-90-5,91673-92-6
D-(+)-galactosamine hydrochloride

: 84278-00-2
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

Guidance literature:: D-(+)-galactosamine hydrochloride; With pyridine; sodium azide; copper(ll) sulfate pentahydrate; trifluoromethylsulfonic anhydride; triethylamine; In water; at 0 ℃; for 48h;

acetic anhydride; With pyridine; dmap; for 2h;
DOI:10.1002/cjoc.202100914