2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole

Base Information

• Chemical Name: 2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole
• CAS No.: 1257408-45-9
• Molecular Formula: C₅₄H₆₀Br₂N₄O₆
• Molecular Weight: 1020.9
• Mol file: 1257408-45-9.mol

Synonyms:2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole

Chemical Property of 2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole

There total 7 articles about 2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.2%

2-(4-hydroxyphenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadiazole (292869-69-3) + 1,4-dibromo-2,5-bis((6-bromohexyl)oxy)benzene (951037-13-1) → 2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole (1257408-45-9)

Guidance literature:

With tetrabutylammomium bromide; sodium hydroxide; In ethanol; dimethyl sulfoxide; at 90 ℃; for 6h;

DOI:10.1016/j.polymer.2010.09.046

Reference yield:

1 ,6-dibromohexane (629-03-8) → 2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole (1257408-45-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 4 h / 90 °C

2: bromine / dichloromethane / 18 h / 0 - 20 °C

3: tetrabutylammomium bromide; sodium hydroxide / ethanol; dimethyl sulfoxide / 6 h / 90 °C

With tetrabutylammomium bromide; bromine; sodium hydroxide; In ethanol; dichloromethane; dimethyl sulfoxide;

DOI:10.1016/j.polymer.2010.09.046

Reference yield:

4-tert-butyl-N'-(4-hydroxybenzoyl)benzohydrazide (319924-12-4) → 2-(4-6-(5-bromo-4-(6-(4-(5-(4-(2-bromopropan-2-yl)phenyl)-(1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)-2-methylphenoxy)hexyloxy)phenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadizaole (1257408-45-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; thionyl chloride / 6 h / 88 °C

2: tetrabutylammomium bromide; sodium hydroxide / ethanol; dimethyl sulfoxide / 6 h / 90 °C

With pyridine; thionyl chloride; tetrabutylammomium bromide; sodium hydroxide; In ethanol; dimethyl sulfoxide;

DOI:10.1016/j.polymer.2010.09.046

upstream raw materials:

1 ,6-dibromohexane

2-(4-hydroxyphenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadiazole

1,4-dibromo-2,5-bis((6-bromohexyl)oxy)benzene

4-tert-butyl-N'-(4-hydroxybenzoyl)benzohydrazide