3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

Base Information

Chemical Name:3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester
CAS No.:1276577-48-0
Molecular Formula:C₂₉H₂₉NO₅S
Molecular Weight:503.619
Hs Code.:

Synonyms:3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

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Chemical Property of 3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

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Technology Process of 3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

There total 9 articles about 3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1116669-89-6
C₁₉H₁₉NO₄S

: 20452-67-9
phenylethylketene

: 1276577-48-0
3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

Guidance literature:: C₁₉H₁₉NO₄S; phenylethylketene; With (5aR,10bS)-2-phenyl-4,5a,6,10b-tetrahydroindeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]-oxazin-2-ium tetrafluoroborate; caesium carbonate; In benzene; at 20 ℃; for 13h; Inert atmosphere;

In 1,2-dimethoxyethane; benzene; at 20 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c0cc04839a

Reference yield:

: 1116669-89-6
C₁₉H₁₉NO₄S

: 20452-67-9
phenylethylketene

: 1276577-48-0
3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

: 1276577-75-3
3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

Guidance literature:: C₁₉H₁₉NO₄S; phenylethylketene; With (S)-5-{[(tert-butyldimethylsilyl)oxy]diphenylmethyl}-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; caesium carbonate; In toluene; at 20 ℃; Inert atmosphere;

In 1,2-dimethoxyethane; toluene; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c0cc04839a

Reference yield:

: 1116669-89-6
C₁₉H₁₉NO₄S

: 20452-67-9
phenylethylketene

: 3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

: 1276577-48-0
3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

: 1276577-75-3
3-ethyl-2-oxo-3,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydropyridine-4-carboxylic acid ethyl ester

Guidance literature:: With (S)-5-{[(tert-butyldimethylsilyl)oxy]diphenylmethyl}-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; caesium carbonate; In toluene; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c0cc04839a