1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

Base Information

Chemical Name:1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine
CAS No.:76166-07-9
Molecular Formula:C₃₀H₄₆N₂O₅Si
Molecular Weight:542.791
Hs Code.:

Synonyms:1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

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Chemical Property of 1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

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Technology Process of 1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

There total 8 articles about 1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 76145-20-5
1,3-diphenyl-2-(3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

: 76166-07-9
1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; Ambient temperature;

Reference yield:

: 28436-51-3
3,5,6-tri-O-methyl-D-glucofuranose

: 76166-07-9
1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / pyridine / 1.) 1 h, 0 deg C, 2.) 2 d, -10 deg C

2: hydrogen bromide / benzene / 0.5 h / 0 °C

3: nitromethane / 20 h / Ambient temperature

4: 62 percent / 0.097 N aqu. sodium hydroxide / tetrahydrofuran

5: 70 percent / Raney nickel, sodium hypophosphite / pyridine; acetic acid; H₂O / 1.25 h / Ambient temperature

6: 80 percent / imidazole / dimethylformamide / Ambient temperature

With pyridine; 1H-imidazole; sodium hydroxide; sodium hypophosphite; hydrogen bromide; nickel; In tetrahydrofuran; pyridine; nitromethane; water; acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 76145-19-2
3,5,6-tri-O-methyl-β-D-glucofuranosyl cyanide

: 76166-07-9
1,3-diphenyl-2-(2-O-(tert-butyldimethyl)silyl-3,5,6-tri-O-methyl-β-D-glucofuranosyl)imidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Raney nickel, sodium hypophosphite / pyridine; acetic acid; H₂O / 1.25 h / Ambient temperature

2: 80 percent / imidazole / dimethylformamide / Ambient temperature

With 1H-imidazole; sodium hypophosphite; nickel; In pyridine; water; acetic acid; N,N-dimethyl-formamide;