C₂₀H₁₅FN₂O

Base Information

Chemical Name:C₂₀H₁₅FN₂O
CAS No.:1590408-76-6
Molecular Formula:C₂₀H₁₅FN₂O
Molecular Weight:318.35
Hs Code.:

C<sub>20</sub>H<sub>15</sub>FN<sub>2</sub>O

Synonyms:C₂₀H₁₅FN₂O

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Chemical Property of C₂₀H₁₅FN₂O

Chemical Property:

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Technology Process of C₂₀H₁₅FN₂O

There total 7 articles about C₂₀H₁₅FN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1590409-86-1
C₂₀H₁₄ClFN₂

: 1590408-76-6
C₂₀H₁₅FN₂O

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium hydroxide; tert-butyl XPhos; In 1,4-dioxane; water; for 10h; Inert atmosphere; Reflux;

Reference yield:

: 6332-56-5
2-hydroxy-3-nitropyridine

: 1590408-76-6
C₂₀H₁₅FN₂O

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; sulfuric acid; periodic acid / water / 0.25 h / 90 °C

1.2: 0.33 h

2.1: O-phenyl phosphorodichloridate / 0.5 h / 180 °C

3.1: tetrahydrofuran; 2-methyltetrahydrofuran / 1.25 h / -70 °C / Inert atmosphere

4.1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / Reflux

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

5.2: 16 h / 20 °C

6.1: tert-butyl XPhos; potassium hydroxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / water; 1,4-dioxane / 10 h / Inert atmosphere; Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; sodium hydride; potassium carbonate; acetic acid; O-phenyl phosphorodichloridate; periodic acid; potassium hydroxide; tert-butyl XPhos; In tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 426463-05-0
2-chloro-5-iodo-3-nitro-pyridine

: 1590408-76-6
C₂₀H₁₅FN₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran; 2-methyltetrahydrofuran / 1.25 h / -70 °C / Inert atmosphere

2.1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

3.2: 16 h / 20 °C

4.1: tert-butyl XPhos; potassium hydroxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / water; 1,4-dioxane / 10 h / Inert atmosphere; Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydride; potassium carbonate; potassium hydroxide; tert-butyl XPhos; In tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;