N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

Base Information

Chemical Name:N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone
CAS No.:122314-18-5
Molecular Formula:C₂₀H₃₁N₅O₅
Molecular Weight:421.497
Hs Code.:

N<sup>α</sup>-(benzyloxycarbonyl)-N<sup>ε</sup>-(tert-butoxycarbonyl)-L-lysinal semicarbazone

Synonyms:N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

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Chemical Property of N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

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Technology Process of N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

There total 1 articles about N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2389-49-3
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysine methyl ester

: 122314-18-5
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminum hydride (DIBAL) / toluene; hexane / 3 h / -50 °C

2: sodium acetate / ethanol; H₂O / 0.75 h / Heating

With sodium acetate; diisobutylaluminium hydride; In ethanol; hexane; water; toluene;
DOI:10.1021/jm00163a014

Reference yield:

: 122314-18-5
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

: 122314-36-7
(benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-lysinal hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

2: triethylamine / CHCl₃ / 3 h / 0 °C

3: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jm00163a014

Reference yield:

: 122314-18-5
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

: 122314-37-8
(benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

2: triethylamine / CHCl₃ / 3 h / 0 °C

3: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jm00163a014