1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

Base Information

Chemical Name:1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate
CAS No.:1196704-30-9
Molecular Formula:C₃₄H₄₅NO₈Si
Molecular Weight:623.819
Hs Code.:

1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

Synonyms:1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

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Chemical Property of 1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

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Technology Process of 1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

There total 1 articles about 1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1196704-28-5
1-benzyl 2-methyl (2S,3S,4R)-4-[2-(benzyloxy)ethyl]-2-formyl-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

: 112520-99-7,1177092-71-5
tributyl(cyclohex-2-en-1-yl)stannane

: 1196704-30-9
1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

Guidance literature:: tributyl(cyclohex-2-en-1-yl)stannane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

With zinc(II) chloride; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

1-benzyl 2-methyl (2S,3S,4R)-4-[2-(benzyloxy)ethyl]-2-formyl-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate; In tetrahydrofuran; hexane; at -78 ℃; for 1h;
DOI:10.1055/s-0029-1216927

Reference yield: 78.0%

: 1196704-30-9
1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate

: 704910-42-9
(2R,3S,4R)-2-((S)-(S)-Cyclohex-2-enyl-hydroxy-methyl)-3-hydroxy-4-(2-hydroxy-ethyl)-3-methyl-5-oxo-pyrrolidine-2-carboxylic acid methyl ester

Guidance literature:: 1-benzyl 2-methyl (2R,3S,4R)-4-[2-(benzyloxy)ethyl]-2-{(S)-[(S)-cyclohex-2-enyl](hydroxy)methyl}-3-methyl-5-oxo-3-trimethylsilyloxypyrrolidine-1,2-dicarboxylate; With boron trichloride; In n-heptane; dichloromethane; at -20 - 0 ℃;

With methanol; In n-heptane; dichloromethane; at 0 ℃;
DOI:10.1055/s-0029-1216927