(S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Base Information

Chemical Name:(S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide
CAS No.:1093169-24-4
Molecular Formula:C₁₉H₃₀N₂O₆
Molecular Weight:382.457
Hs Code.:

Synonyms:(S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Suppliers and Price of (S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

There total 1 articles about (S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1093169-44-8
(S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N-methyltyrosinamide

: 74-88-4
methyl iodide

: 1093169-24-4
(S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at -20 ℃;
DOI:10.1016/j.tetlet.2008.09.141

Reference yield:

: 1093169-24-4
(S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

: 1093169-37-9
C₁₇H₂₅NO₅

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; optical yield given as %ee;
DOI:10.1016/j.tetlet.2008.09.141

Reference yield:

: 1093169-24-4
(S)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

: 832150-38-6
(2S,3R,6E,8R,10R)-1-(4-hydroxyphenyl)-8,10-dimethyl-2-(methylamino)dodec-6-en-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / diethyl ether

2.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / tetrahydrofuran; methanol; water / 4 h / 20 °C

With tert.-butyl lithium; diisobutylaluminium hydride; trifluoroacetic acid; In tetrahydrofuran; methanol; diethyl ether; water; pentane;
DOI:10.1271/bbb.100361