C₂₅H₃₆O₂Si

Base Information

Chemical Name:C₂₅H₃₆O₂Si
CAS No.:1207538-76-8
Molecular Formula:C₂₅H₃₆O₂Si
Molecular Weight:396.645
Hs Code.:

C<sub>25</sub>H<sub>36</sub>O<sub>2</sub>Si

Synonyms:C₂₅H₃₆O₂Si

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Chemical Property of C₂₅H₃₆O₂Si

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Technology Process of C₂₅H₃₆O₂Si

There total 9 articles about C₂₅H₃₆O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1207538-88-2
C₂₇H₃₈O₃Si

: 1207538-76-8
C₂₅H₃₆O₂Si

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.833333h; Inert atmosphere;
DOI:10.1021/ol902960n

Reference yield:

: C₂₉H₄₅O₅PSi

: 1207538-76-8
C₂₅H₃₆O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: C₄₃H₃₅N₂O₃⁽¹⁺⁾*BF₄^(1-); tetrakis(actonitrile)copper(I) hexafluorophosphate; lithium tert-butoxide / tetrahydrofuran / 24 h / -20 °C / Schlenk technique; Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.17 h / -78 °C / Schlenk technique; Inert atmosphere

2.2: 2 h / -78 - 0 °C / Schlenk technique; Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid; sodium acetate / dichloromethane / 3 h / 0 °C

4.1: periodic acid / tetrahydrofuran; diethyl ether / 1 h / 0 °C

5.1: sodium tetrahydroborate; methanol / 1 h / 0 °C

With methanol; sodium tetrahydroborate; tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium acetate; C₄₃H₃₅N₂O₃⁽¹⁺⁾*BF₄^(1-); periodic acid; 3-chloro-benzenecarboperoxoic acid; lithium tert-butoxide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1002/anie.202110709

Reference yield:

: 445424-75-9
ethyl 6-(tert-butyldiphenylsilyloxy)-3-methylhex-2-enoate

: 1207538-76-8
C₂₅H₃₆O₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C

2.1: dmap; triethylamine / dichloromethane / 12 h / 0 - 20 °C

3.1: C₄₃H₃₅N₂O₃⁽¹⁺⁾*BF₄^(1-); tetrakis(actonitrile)copper(I) hexafluorophosphate; lithium tert-butoxide / tetrahydrofuran / 24 h / -20 °C / Schlenk technique; Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.17 h / -78 °C / Schlenk technique; Inert atmosphere

4.2: 2 h / -78 - 0 °C / Schlenk technique; Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid; sodium acetate / dichloromethane / 3 h / 0 °C

6.1: periodic acid / tetrahydrofuran; diethyl ether / 1 h / 0 °C

7.1: sodium tetrahydroborate; methanol / 1 h / 0 °C

With methanol; dmap; sodium tetrahydroborate; tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium acetate; C₄₃H₃₅N₂O₃⁽¹⁺⁾*BF₄^(1-); diisobutylaluminium hydride; periodic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium tert-butoxide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1002/anie.202110709