Re₂Os13COC⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)

Base Information

Chemical Name:Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)
CAS No.:98688-92-7
Molecular Formula:13CO*C₂H₃N*OsRe₂
Molecular Weight:970.778
Hs Code.:

Re<sub>2</sub>Os*13CO*C<sup>(2)</sup>H<sub>3</sub>CN=Re<sub>2</sub>Os(CO)13(C<sup>(2)</sup>H<sub>3</sub>CN)

Synonyms:Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)

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Chemical Property of Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)

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Technology Process of Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)

There total 2 articles about Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 16457-30-0
hydridopentacarbonylrhenium(I)

: 59599-35-8
dimethyl(tetracarbonyl)osmium

: 14285-68-8
decacarbonyldirhenium⁽⁰⁾

: 34557-54-5,27936-85-2
methane

: 98688-84-7
Re₂(CO)9(C⁽²⁾H₃CN)

: 98688-92-7
Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)

: 75-07-0,9002-91-9
acetaldehyde

Guidance literature:: In [D₃]acetonitrile; Me2Os(CO)4, HRe(CO)5 (1:4 molar ratio), and CD3CN were sealed in an NMRtube and heated at 60°C for 10 d; the tube was broken open on the vac. line, volatile components (-196°C) were collected via a Toepler pump, and analysed by GC, nonvolatile residue was subjected to preparative layer chromy.; yield of MeCHO was detd. by (1)H NMR, of CH4 - by GC;

Reference yield: 42.0%

: 16457-30-0
hydridopentacarbonylrhenium(I)

: (CO)4Os(CH₂CH₃)2

: 98688-96-1
C₂H₅Os(CO)4Re(CO)5

: 98688-95-0
C₂H₅C(O)Os(CO)4Re(CO)5

: 98688-92-7
Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)

: 123-38-6
propionaldehyde

Guidance literature:: With CH₃CN; In acetonitrile; byproducts: C2H6; Et2Os(CO)4 and HRe(CO)5 (1:1 molar ratio) were heated in MeCN to 45°C for 20 h; solvent was removed, residue was placed under high vac. overnight and subjected to preparative layer chromy.; elem. anal. for EtOsRe(CO)9;