N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

Base Information

Chemical Name:N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester
CAS No.:1402586-16-6
Molecular Formula:C₁₉H₂₃N₃O₆S
Molecular Weight:421.474
Hs Code.:

Synonyms:N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

Suppliers and Price of N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

There total 8 articles about N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1402586-15-5
tert-butyl N-(4-aminobenzyl)sulfamoyl-carbamate

: 1885-14-9
phenyl chloroformate

: 1402586-16-6
N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

Guidance literature:: With pyridine; In tetrahydrofuran; acetonitrile; at 0 - 20 ℃; for 1h;

Reference yield:

: 99-99-0
1-methyl-4-nitrobenzene

: 1402586-16-6
N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 24 h / Reflux

2.1: N,N-dimethyl-formamide

3.1: hydrazine hydrate / tetrahydrofuran / 6 h / Reflux

4.1: dichloromethane / 0.17 h

4.2: 0.5 h / 50 °C

4.3: 3 h / 20 °C

5.1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; ethanol / 6 h / 20 °C

6.1: pyridine / tetrahydrofuran; acetonitrile / 1 h / 0 - 20 °C

With pyridine; N-Bromosuccinimide; palladium 10% on activated carbon; hydrogen; hydrazine hydrate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1402586-16-6
N-[4-[[(tert-butoxycarbonyl-sulfamoyl)amino]-methyl]-phenyl]-carbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide

2.1: hydrazine hydrate / tetrahydrofuran / 6 h / Reflux

3.1: dichloromethane / 0.17 h

3.2: 0.5 h / 50 °C

3.3: 3 h / 20 °C

4.1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; ethanol / 6 h / 20 °C

5.1: pyridine / tetrahydrofuran; acetonitrile / 1 h / 0 - 20 °C

With pyridine; palladium 10% on activated carbon; hydrogen; hydrazine hydrate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;