4-(phenylsulphonyloxy)benzyl benzenesulphonate

Base Information

Chemical Name:4-(phenylsulphonyloxy)benzyl benzenesulphonate
CAS No.:74454-32-3
Molecular Formula:C₁₉H₁₆O₆S₂
Molecular Weight:404.464
Hs Code.:

Synonyms:4-(phenylsulphonyloxy)benzyl benzenesulphonate

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Chemical Property of 4-(phenylsulphonyloxy)benzyl benzenesulphonate

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Technology Process of 4-(phenylsulphonyloxy)benzyl benzenesulphonate

There total 4 articles about 4-(phenylsulphonyloxy)benzyl benzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 118107-84-9
Benzenesulfonic acid 4-hydroxymethyl-phenyl ester

: 98-09-9
benzenesulfonyl chloride

: 74454-32-3
4-(phenylsulphonyloxy)benzyl benzenesulphonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 10 ℃; for 2h;

Reference yield:

: 13493-50-0
4-hydroxybenzaldehyde benzenesulfonate ester

: 74454-32-3
4-(phenylsulphonyloxy)benzyl benzenesulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 460 mg / sodium borohydride / methanol / 3 h / 20 °C

2: 43 percent / triethylamine / CH₂Cl₂ / 2 h / 0 - 10 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 74454-32-3
4-(phenylsulphonyloxy)benzyl benzenesulphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / triethylamine / CH₂Cl₂ / 0.25 h / 0 - 10 °C

2: 460 mg / sodium borohydride / methanol / 3 h / 20 °C

3: 43 percent / triethylamine / CH₂Cl₂ / 2 h / 0 - 10 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;