2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester

Base Information

Chemical Name:2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester
CAS No.:155526-48-0
Molecular Formula:C₂₆H₃₈N₂O₇
Molecular Weight:490.597
Hs Code.:

Synonyms:2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester

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Chemical Property of 2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester

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Technology Process of 2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester

There total 6 articles about 2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623-27-8
terephthalaldehyde,

: 155526-48-0
2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 25.2 g / H₂ / 10percent Pd/C / ethanol; H₂O / 3 h / 760 Torr / Ambient temperature

2: 82 percent / 48percent aq. HBr / toluene / 2 h / Heating

3: 74 percent / KNO₃, H₂SO₄ / 4 h / Ambient temperature

4: 98 percent / NaH / dimethylformamide / 2.5 h / Ambient temperature

5: 1.) n-BuLi / 1.) THF, 0 deg C, 90 min, 2.) THF, a) -78 deg C, 90 min, b) 0 deg C, 2 h

With n-butyllithium; sulfuric acid; hydrogen bromide; hydrogen; sodium hydride; potassium nitrate; palladium on activated charcoal; In ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja953578v

Reference yield:

: 155526-65-1
4-(bromomethyl)-3-nitrobenzaldehyde

: 155526-48-0
2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaH / dimethylformamide / 2.5 h / Ambient temperature

2: 1.) n-BuLi / 1.) THF, 0 deg C, 90 min, 2.) THF, a) -78 deg C, 90 min, b) 0 deg C, 2 h

With n-butyllithium; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/ja953578v

Reference yield:

: 51359-78-5
4-(bromomethyl)benzaldehyde

: 155526-48-0
2-Acetylamino-2-[4-((E)-dec-1-enyl)-2-nitro-benzyl]-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / KNO₃, H₂SO₄ / 4 h / Ambient temperature

2: 98 percent / NaH / dimethylformamide / 2.5 h / Ambient temperature

3: 1.) n-BuLi / 1.) THF, 0 deg C, 90 min, 2.) THF, a) -78 deg C, 90 min, b) 0 deg C, 2 h

With n-butyllithium; sulfuric acid; sodium hydride; potassium nitrate; In N,N-dimethyl-formamide;
DOI:10.1021/ja953578v