Technology Process of (C6H5)2C3H3C2H4O
There total 6 articles about (C6H5)2C3H3C2H4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 98 percent / LiAlH4 / diethyl ether / 0.75 h / 20 °C
2.1: 92 percent / PCC / CH2Cl2 / 2.5 h / 20 °C
3.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 20 °C
3.2: 79 percent / HCl / tetrahydrofuran; H2O / 2.5 h / Heating
4.1: 99 percent / LiAlH4 / diethyl ether / 0.33 h / 20 °C
5.1: 75 percent / Et3N / CH2Cl2 / 0.42 h / 0 - 20 °C
6.1: acetonitrile / 22 °C / Photolysis
With
lithium aluminium tetrahydride; triethylamine; pyridinium chlorochromate; lithium hexamethyldisilazane;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo026218g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 20 °C
1.2: 79 percent / HCl / tetrahydrofuran; H2O / 2.5 h / Heating
2.1: 99 percent / LiAlH4 / diethyl ether / 0.33 h / 20 °C
3.1: 75 percent / Et3N / CH2Cl2 / 0.42 h / 0 - 20 °C
4.1: acetonitrile / 22 °C / Photolysis
With
lithium aluminium tetrahydride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo026218g