C₆₅H₉₄O₁₀Si₂

Base Information

Chemical Name:C₆₅H₉₄O₁₀Si₂
CAS No.:220691-31-6
Molecular Formula:C₆₅H₉₄O₁₀Si₂
Molecular Weight:1091.63
Hs Code.:

C<sub>65</sub>H<sub>94</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₆₅H₉₄O₁₀Si₂

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Chemical Property of C₆₅H₉₄O₁₀Si₂

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Technology Process of C₆₅H₉₄O₁₀Si₂

There total 34 articles about C₆₅H₉₄O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 220691-95-2
C₅₆H₇₄O₁₀Si

: 220691-31-6
C₆₅H₉₄O₁₀Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane;

Reference yield:

: 52813-63-5
(5R)-2,3,4,5-tetrahydro-5-hydroxymethyl-2-furanone

: 220691-31-6
C₆₅H₉₄O₁₀Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: 84 percent / Ph₃P, DEAD / tetrahydrofuran / Heating

2: 98 percent / DIBAL-H / toluene / -78 °C

3: acetonitrile

4: NaOH / H₂O / Heating

5: 1.) LDA, 2.) t-BuOK / 1.) THF, -78 deg C, 2.) THF, -78 deg C to r.t.

6: H₂O, TFA / CH₂Cl₂

7: 87 percent / imidazole / dimethylformamide

8: 96 percent / MCPBA, NaOAc / CH₂Cl₂ / 0 °C

9: 1.) BuLi, Me₂AlCl / 1.) PhMe, 0 deg C; CH₂Cl₂, 0 deg C to r.t., 2.) PhMe, CH₂Cl₂

10: 1.) 9-BBN, 2.) NaOH, H₂O₂ / 1.) THF, reflux, 2.) THF, H₂O₂, r.t.

11: NaBH₄ / ethanol / 0 °C

12: 95 percent / 2,6-lutidine / CH₂Cl₂

With 1H-imidazole; 2,6-dimethylpyridine; sodium hydroxide; sodium tetrahydroborate; 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; potassium tert-butylate; water; dihydrogen peroxide; sodium acetate; dimethylaluminum chloride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 100-39-0
benzyl bromide

: 220691-31-6
C₆₅H₉₄O₁₀Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: 95 percent / NaH / dimethylformamide

2: Et₃N / CH₂Cl₂ / -78 °C

3: dimethylformamide; acetonitrile

4: 90 percent / DIBAL-H / toluene / -78 °C

5: 1.) LDA, 2.) t-BuOK / 1.) THF, -78 deg C, 2.) THF, -78 deg C to r.t.

6: H₂O, TFA / CH₂Cl₂

7: 87 percent / imidazole / dimethylformamide

8: 96 percent / MCPBA, NaOAc / CH₂Cl₂ / 0 °C

9: 1.) BuLi, Me₂AlCl / 1.) PhMe, 0 deg C; CH₂Cl₂, 0 deg C to r.t., 2.) PhMe, CH₂Cl₂

10: 1.) 9-BBN, 2.) NaOH, H₂O₂ / 1.) THF, reflux, 2.) THF, H₂O₂, r.t.

11: NaBH₄ / ethanol / 0 °C

12: 95 percent / 2,6-lutidine / CH₂Cl₂

With 1H-imidazole; 2,6-dimethylpyridine; sodium hydroxide; sodium tetrahydroborate; 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; potassium tert-butylate; water; dihydrogen peroxide; sodium acetate; dimethylaluminum chloride; sodium hydride; diisobutylaluminium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; lithium diisopropyl amide; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;