2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1132094-49-5
Molecular Formula:C₁₆H₂₅BO₆
Molecular Weight:324.182
Hs Code.:

Synonyms:2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 3 articles about 2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1132094-48-4
4-bromo-1,2-bis(methoxymethoxy)benzene

: 73183-34-3
bis(pinacol)diborane

: 1132094-49-5
2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 15h;
DOI:10.1039/c4ta01286k

Reference yield:

: 17345-77-6
1-bromo-3,4-dihydroxybenzene

: 1132094-49-5
2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 14 h / 20 °C / Inert atmosphere

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 15 h / 80 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c4ta01286k

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: C₁₂H₁₉BO₆

: 1132094-49-5
2-[3,4-bis(methoxymethoxy)-phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 2,3-dimethyl-2,3-butane diol; C₁₂H₁₉BO₆; In tetrahydrofuran; hexane; for 1h; Inert atmosphere;

With acetic acid; In tetrahydrofuran; hexane; Inert atmosphere;
DOI:10.1039/b814536a