N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester

Base Information

• Chemical Name: N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester
• CAS No.: 96866-16-9
• Molecular Formula: C₂₇H₂₈N₂O₅
• Molecular Weight: 460.53

Synonyms:N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester

Chemical Property of N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester

Chemical Property:

Purity/Quality:

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Technology Process of N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester

There total 3 articles about N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyloxyamine (622-33-3) → N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester (96866-16-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 57 percent / ethanol / 168 h / Heating

2: 98 percent / acetic anhydride / 3 h / 0 °C

3: 97 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

With acetic anhydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform;

DOI:10.1021/jm00147a007

Reference yield:

2-Benzyl-2-propenoic acid (5669-19-2) → N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester (96866-16-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 57 percent / ethanol / 168 h / Heating

2: 98 percent / acetic anhydride / 3 h / 0 °C

3: 97 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

With acetic anhydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform;

DOI:10.1021/jm00147a007

Reference yield:

2-(R,S)-benzyl-3-benzyloxyamino-propionic acid (96866-14-7) → N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzyl ester (96866-16-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / acetic anhydride / 3 h / 0 °C

2: 97 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

With acetic anhydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform;

DOI:10.1021/jm00147a007

upstream raw materials:

N-benzyloxyamine

2-Benzyl-2-propenoic acid

2-(R,S)-benzyl-3-benzyloxyamino-propionic acid

Downstream raw materials:

N-(N-hydroxy 3-formamido 2-benzyl propanoyl)-glycine

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