2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole

Base Information

Chemical Name:2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole
CAS No.:475475-59-3
Molecular Formula:C₂₂H₁₉N₂O₂P
Molecular Weight:374.379
Hs Code.:

Synonyms:2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole

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Technology Process of 2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole

There total 1 articles about 2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 118482-08-9
1-vinylbenzimidazole-2-carboxaldehyde

: 4559-70-0
Diphenylphosphine oxide

: 475475-59-3
2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole

Guidance literature:: 99; In 1,4-dioxane; at 20 ℃; for 1h;
DOI:10.1023/A:1014855309771

Reference yield: 80.0%

: 10108-64-2
cadmium(II) chloride

: 475475-59-3
2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole

: 868261-39-6
CdCl₂(2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole)2

Guidance literature:: In ethanol; stirring of CdCl2 (1 equiv.) and 2-((diphenylphosphinoyl)hydroxymethyl)-1-vinylbenzimidazole (2 equiv.) in abs. EtOH at 60°C for 8-15 h; pptn. with ether, drying, elem. anal.;
DOI:10.1007/s11176-005-0198-x

Reference yield: 42.0%

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 475475-59-3
2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole

: 868261-44-3
CoCl(2-[(diphenylphosphinoyl)hydroxymethyl]-1-vinylbenzimidazole(-1H))

Guidance literature:: In ethanol; stirring of CoCl2 and 2-((diphenylphosphinoyl)hydroxymethyl)-1-vinylbenzimidazole in abs. EtOH at 60°C for 8-15 h; pptn. with ether, drying, elem. anal.;
DOI:10.1007/s11176-005-0198-x