N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide

Base Information

Chemical Name:N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide
CAS No.:1421851-56-0
Molecular Formula:C₁₂H₁₀N₂O₄
Molecular Weight:246.222
Hs Code.:

Synonyms:N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide

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Technology Process of N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide

There total 1 articles about N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 6118-51-0
exo-3,6-epoxy-1,2,3,6-tetrahydrophthalic anhydride

: 14678-02-5
5-amino-3-methylisoxazole

: 1421851-56-0
N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide

Guidance literature:: With acetic acid; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1080/00304948.2013.743423

Reference yield: 70.0%

: 637-87-6
1-Chloro-4-iodobenzene

: 1421851-56-0
N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide

: N-(3-methylisoxazol-5-yl)-5-exo-(4-chlorophenyl)-7-oxabicyclo[2.2.1]heptane-2-exo,3-exo-dicarboximide

Guidance literature:: With formic acid; triphenyl-arsane; palladium diacetate; triethylamine; In N,N-dimethyl-formamide; at 65 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1080/00304948.2013.743423

Reference yield: 60.0%

: 1421851-56-0
N-(3-methylisoxazol-5-yl)-7-oxabicyclo[2.2.1]hept-5-ene-2-exo,3-exo-dicarboximide

: 67184-41-2,34967-19-6
2,5‐dimethoxybenzaldoxime

: 4,8-epoxy-3-(2,5-dimethoxyphenyl)-6-(3-methylisoxazol-5-yl)-4,4a,8,exo-8a-tetrahydro-exo-3aH-isoxazolo[5,4-f]isoindole-5,7(6H,7aH)-exo-dione

Guidance literature:: With sodium hypochlorite; In dichloromethane; water; at 0 - 20 ℃; for 8h; Inert atmosphere;
DOI:10.1080/00304948.2013.743423