ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate

Base Information

Chemical Name:ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate
CAS No.:1335145-66-8
Molecular Formula:C₂₆H₃₄N₂O₃
Molecular Weight:422.568
Hs Code.:

Synonyms:ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate

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Chemical Property of ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate

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Technology Process of ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate

There total 3 articles about ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 286946-67-6
benzyl 2,6-diazabicyclo[3.2.1]-octane-6-carboxylate

: 1335145-66-8
ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 130 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 3 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / dichloromethane / 20 °C

With hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; palladium 10% on activated carbon; In methanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1335145-64-6
benzyl 2-(4-(ethoxycarbonyl)phenyl)-2,6-diazabicyclo[3.2.1]octane-6-carboxylate

: 1335145-66-8
ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 3 h

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / dichloromethane / 20 °C

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; palladium 10% on activated carbon; In methanol; dichloromethane;

Reference yield:

: 451-46-7
4-fluorobenzoic acid ethyl ester

: 1335145-66-8
ethyl 4-{6-[adamantan-1-ylcarbonyl]-2,6-diazabicyclo[3.2.1]oct-2-yl}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 130 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 3 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / dichloromethane / 20 °C

With hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; palladium 10% on activated carbon; In methanol; dichloromethane; dimethyl sulfoxide;