Technology Process of C40H46O8
There total 5 articles about C40H46O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid; orthoformic acid triethyl ester;
at 20 ℃;
for 3h;
DOI:10.1016/j.bmc.2012.03.001
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine; dmap / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
2: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
3: periodic acid / methanol / 1 h / 20 °C
4: barium carbonate; pyridinium chlorochromate / dichloromethane / 20 h / 20 °C
5: toluene-4-sulfonic acid; orthoformic acid triethyl ester / 3 h / 20 °C
With
pyridine; dmap; toluene-4-sulfonic acid; periodic acid; lithium tri-t-butoxyaluminum hydride; orthoformic acid triethyl ester; barium carbonate; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmc.2012.03.001
- Guidance literature:
-
Multi-step reaction with 3 steps
1: periodic acid / methanol / 1 h / 20 °C
2: barium carbonate; pyridinium chlorochromate / dichloromethane / 20 h / 20 °C
3: toluene-4-sulfonic acid; orthoformic acid triethyl ester / 3 h / 20 °C
With
toluene-4-sulfonic acid; periodic acid; orthoformic acid triethyl ester; barium carbonate; pyridinium chlorochromate;
In
methanol; dichloromethane;
DOI:10.1016/j.bmc.2012.03.001
