2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate

Base Information

Chemical Name:2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate
CAS No.:153895-18-2
Molecular Formula:C₄₆H₅₄O₅S
Molecular Weight:718.998
Hs Code.:

Synonyms:2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate

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Technology Process of 2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate

There total 9 articles about 2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 98-59-9
p-toluenesulfonyl chloride

: 177609-52-8
2-(2-{4-[bis(4-tert-butylphenyl)-(4-ethylphenyl)methyl]phenoxy}ethoxy)ethanol

: 153895-18-2
2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate

Guidance literature:: With sodium hydroxide; benzyltriethylammonium bromide; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1021/ja954334d

Reference yield:

: 392711-10-3
bis(4-tert-butylphenyl)(4-ethylphenyl)methanol

: 153895-18-2
2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / aq. HCl / 4 h / Heating

2: KOH; LiBr / butan-1-ol / 60 h / Heating

3: 9.90 g / aq. HCl / methanol; CH₂Cl₂ / 2.5 h / 20 °C

4: 53 percent / NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; butan-1-ol;
DOI:10.1021/ja0114456

Reference yield:

: 177609-49-3
bis(4-tert-butylphenyl)(4-ethylphenyl)(4-hydroxyphenyl)methane

: 153895-18-2
2-{4-[4-Ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy}ethoxy ethanol 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: KOH; LiBr / butan-1-ol / 60 h / Heating

2: 9.90 g / aq. HCl / methanol; CH₂Cl₂ / 2.5 h / 20 °C

3: 53 percent / NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; butan-1-ol;
DOI:10.1021/ja0114456