N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

Base Information

Chemical Name:N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam
CAS No.:310896-89-0
Molecular Formula:C₂₂H₃₅NOSi₂
Molecular Weight:385.697
Hs Code.:

Synonyms:N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

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Chemical Property of N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

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Technology Process of N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

There total 3 articles about N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 310896-83-4
3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

: 310896-89-0
N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

Guidance literature:: With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; at -20 ℃; for 4h;
DOI:10.1021/ol0065221

Reference yield:

: 66224-70-2
3-(trimethylsilyl)propynoyl chloride

: 310896-89-0
N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

Guidance literature:: Multi-step reaction with 2 steps

2: 83 percent / Ti(O-i-Pr)4; i-PrMgCl / diethyl ether / 4 h / -20 °C

With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; 1: Acylation / 2: Cyclization;
DOI:10.1021/ol0065221

Reference yield:

: 392232-53-0
benzyl-[1-isopropyl-3-(trimethyl-silanyl)-prop-2-ynyl]-amine

: 310896-89-0
N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

Guidance literature:: Multi-step reaction with 2 steps

2: 83 percent / Ti(O-i-Pr)4; i-PrMgCl / diethyl ether / 4 h / -20 °C

With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; 1: Acylation / 2: Cyclization;
DOI:10.1021/ol0065221