3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

Base Information

Chemical Name:3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide
CAS No.:310896-83-4
Molecular Formula:C₂₂H₃₃NOSi₂
Molecular Weight:383.681
Hs Code.:

Synonyms:3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

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Chemical Property of 3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

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Technology Process of 3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

There total 1 articles about 3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66224-70-2
3-(trimethylsilyl)propynoyl chloride

: 392232-53-0
benzyl-[1-isopropyl-3-(trimethyl-silanyl)-prop-2-ynyl]-amine

: 310896-83-4
3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

Guidance literature:: DOI:10.1021/ol0065221

Reference yield: 83.0%

: 310896-83-4
3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

: 310896-89-0
N-benzyl-2,3-bis[(Z)-(trimethylsilyl)methylidene]-4-isopropyl-4-butanelactam

Guidance literature:: With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; at -20 ℃; for 4h;
DOI:10.1021/ol0065221

Reference yield:

: 310896-83-4
3-trimethylsilanyl-propynoic acid benzyl-(1-isopropyl-3-trimethylsilanyl-prop-2-ynyl)-amide

: (3aR,4S,7S,8R,8aS)-6-Benzyl-7-isopropyl-2-phenyl-4,8-bis-trimethylsilanyl-3a,4,6,7,8,8a-hexahydro-pyrrolo[3,4-f]isoindole-1,3,5-trione

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Ti(O-i-Pr)4; i-PrMgCl / diethyl ether / 4 h / -20 °C

2: 95 percent / toluene / Heating

With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; toluene; 1: Cyclization / 2: Diels-Alder reaction;
DOI:10.1021/ol0065221