C₁₄H₈SO₂P(O)Ph

Base Information

Chemical Name:C₁₄H₈SO₂P(O)Ph
CAS No.:1263143-09-4
Molecular Formula:C₂₀H₁₃O₃PS
Molecular Weight:364.361
Hs Code.:

C<sub>14</sub>H<sub>8</sub>SO<sub>2</sub>P(O)Ph

Synonyms:C₁₄H₈SO₂P(O)Ph

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Chemical Property of C₁₄H₈SO₂P(O)Ph

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Technology Process of C₁₄H₈SO₂P(O)Ph

There total 6 articles about C₁₄H₈SO₂P(O)Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1263143-06-1
10-phenyl-10-oxo-[1]benzophospholo[3,2-b][1]benzothiophene

: 1263143-09-4
C₁₄H₈SO₂P(O)Ph

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1021/ja108081b

Reference yield:

: 1263143-03-8
3-bromo-2-(2-bromophenyl)benzo[b]thiophene

: 1263143-09-4
C₁₄H₈SO₂P(O)Ph

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: dihydrogen peroxide / dichloromethane / 20 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 72 h / 20 °C / Inert atmosphere

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dihydrogen peroxide; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1021/ja108081b

Reference yield:

: 6287-82-7
2,3-dibromobenzo[b]thiophene

: 1263143-09-4
C₁₄H₈SO₂P(O)Ph

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide / tetrahydrofuran; water / 48 h / Reflux; Inert atmosphere

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: dihydrogen peroxide / dichloromethane / 20 °C / Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 72 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dihydrogen peroxide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; 1.1: Suzuki coupling;
DOI:10.1021/ja108081b