1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol

Base Information

Chemical Name:1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol
CAS No.:135892-96-5
Molecular Formula:C₂₈H₃₄O₃Si
Molecular Weight:446.662
Hs Code.:

Synonyms:1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol

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Chemical Property of 1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol

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Technology Process of 1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol

There total 5 articles about 1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132-64-9,214827-48-2
dibenzofuran

: 135892-96-5
1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 82.5 percent / Br₂ / acetic acid / Ambient temperature

2: 71 percent / AlCl₃ / CS₂

3: 97 percent / NaBH₄ / propan-2-ol; H₂O / 1 h / Heating

4: 99 percent / imidazole / dimethylformamide / 20 h

5: 1.) EtMgBr, Mg / 1.) THF, 65 deg C, 90 min, 2.) THF, room temperature, 20 h

With 1H-imidazole; sodium tetrahydroborate; aluminium trichloride; ethylmagnesium bromide; bromine; magnesium; In carbon disulfide; water; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo960330v

Reference yield:

: 86-76-0
2-bromodibenzo[b,d]furan

: 135892-96-5
1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / AlCl₃ / CS₂

2: 97 percent / NaBH₄ / propan-2-ol; H₂O / 1 h / Heating

3: 99 percent / imidazole / dimethylformamide / 20 h

4: 1.) EtMgBr, Mg / 1.) THF, 65 deg C, 90 min, 2.) THF, room temperature, 20 h

With 1H-imidazole; sodium tetrahydroborate; aluminium trichloride; ethylmagnesium bromide; magnesium; In carbon disulfide; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo960330v

Reference yield:

: 135892-93-2
2-bromo-8-(phenylacetyl)dibenzofuran

: 135892-96-5
1-{8-[1-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-ethyl]-dibenzofuran-2-yl}-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaBH₄ / propan-2-ol; H₂O / 1 h / Heating

2: 99 percent / imidazole / dimethylformamide / 20 h

3: 1.) EtMgBr, Mg / 1.) THF, 65 deg C, 90 min, 2.) THF, room temperature, 20 h

With 1H-imidazole; sodium tetrahydroborate; ethylmagnesium bromide; magnesium; In water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo960330v