Technology Process of 4-<2-(N-tert-butoxycarbonyl)aminoethyl>-1,2-diacetamidobenzene
There total 7 articles about 4-<2-(N-tert-butoxycarbonyl)aminoethyl>-1,2-diacetamidobenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 57 percent / pyridine / acetic acid / 2 h / Heating
2: 43 percent / HNO3, conc. H2SO4 / acetic anhydride / 4 h, 0 deg C; 20 h, RT
3: 92 percent / 6 N HCl / 4 h / Heating
4: 93 percent / 1.0 N NaOH / dioxane; H2O / 0.5 h / Ambient temperature
5: hydrazine hydrate / Ra-Ni / ethanol; 1,2-dichloro-ethane / 1 h / Heating
6: 48 percent / pyridine / Ambient temperature
With
pyridine; hydrogenchloride; sodium hydroxide; sulfuric acid; nitric acid; hydrazine hydrate;
Ra-Ni;
In
1,4-dioxane; ethanol; water; acetic anhydride; acetic acid; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / 1.0 N NaOH / dioxane; H2O / 0.5 h / Ambient temperature
2: hydrazine hydrate / Ra-Ni / ethanol; 1,2-dichloro-ethane / 1 h / Heating
3: 48 percent / pyridine / Ambient temperature
With
pyridine; sodium hydroxide; hydrazine hydrate;
Ra-Ni;
In
1,4-dioxane; ethanol; water; 1,2-dichloro-ethane;
