N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine
CAS No.:1071051-66-5
Molecular Formula:C₂₀H₂₅NO₅S
Molecular Weight:391.488
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine

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Chemical Property of N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine

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Technology Process of N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine

There total 1 articles about N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4248-19-5
tert-butyl carbazate

: 824-79-3
sodium 4-methylbenzenesulfinate

: 135-02-4
ortho-anisaldehyde

: 1071051-66-5
N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine

Guidance literature:: With formic acid; In methanol; water; at 20 ℃; for 72h;
DOI:10.1002/adsc.200800214

Reference yield: 84.0%

: 1071051-66-5
N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine

: 850210-37-6
ethyl 3-(2-formylphenoxy)acrylate

: ethyl (2SR, 1RS)-2-[(tert-butoxycarbonylamino)(orthomethoxyphenyl)methyl]benzofuran-3-one-2-acetate

Guidance literature:: With 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; caesium carbonate; In benzene; for 10h; Inert atmosphere; Reflux;
DOI:10.1002/adsc.201400331

Reference yield: 83.0%

: 1071051-66-5
N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-2-methoxybenzylamine

: 86867-62-1,91388-37-3
(E)-3-(2-formylphenyl)propenoic acid ethyl ester

: C₂₅H₂₉NO₆

Guidance literature:: With caesium carbonate; 3-benzyl-4,5-dimethylthiazol-3-ium bromide; In dichloromethane; at 20 ℃; for 5h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c0cc01769h