1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one

Base Information

Chemical Name:1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one
CAS No.:1432044-45-5
Molecular Formula:C₂₃H₂₀N₄O
Molecular Weight:368.438
Hs Code.:

Synonyms:1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one

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Chemical Property of 1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one

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Technology Process of 1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one

There total 2 articles about 1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1432044-51-3
C₁₅H₁₄N₄

: 99-91-2
para-chloroacetophenone

: 1432044-45-5
1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one

Guidance literature:: With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; N-(tert-butylcarbonyl)-L-valine; potassium carbonate; In 1,4-dioxane; at 140 ℃; for 24h; Reagent/catalyst; chemoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201600742

Reference yield: 65.0%

: 1432044-51-3
C₁₅H₁₄N₄

: 99-90-1
para-bromoacetophenone

: 1432044-45-5
1-{2'-(1-benzyl-1H-tetrazol-5-yl)-4'-methyl-[1,1'-biphenyl]-4-yl}ethan-1-one

Guidance literature:: With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; mesitylenecarboxylic acid; potassium carbonate; In toluene; at 120 ℃; for 18h; chemoselective reaction;
DOI:10.1016/j.tet.2013.01.006