5-Ethyl-3-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-[1,3,4]thiadiazol-2-ylideneamine

Base Information

• Chemical Name: 5-Ethyl-3-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-[1,3,4]thiadiazol-2-ylideneamine
• CAS No.: 167005-94-9
• Molecular Formula: C₁₈H₁₇N₇S
• Molecular Weight: 363.446

Synonyms:5-Ethyl-3-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-[1,3,4]thiadiazol-2-ylideneamine

Chemical Property of 5-Ethyl-3-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-[1,3,4]thiadiazol-2-ylideneamine

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Technology Process of 5-Ethyl-3-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-[1,3,4]thiadiazol-2-ylideneamine

There total 8 articles about 5-Ethyl-3-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-[1,3,4]thiadiazol-2-ylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

5-ethyl-2-imino-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline (185515-83-7) + butan-1-ol (71-36-3) → 5-ethyl-2-imino-3-[2'-(1H-tetrazol-5-yl)-biphenyl-4-yl]methyl-1,3,4-thiadiazoline (167005-94-9)

Guidance literature:

With sodium hydroxide; sulfuric acid; Zinc chloride; In chloroform; water;

Reference yield:

2-Acetylimino-5-ethyl-3-[2'-(1H-tetrazol-5-yl)-biphenyl-4-yl]methyl-1,3,4-thiadiazoline → 5-ethyl-2-imino-3-[2'-(1H-tetrazol-5-yl)-biphenyl-4-yl]methyl-1,3,4-thiadiazoline (167005-94-9)

Guidance literature:

With sodium hydroxide; In ethanol; di-isopropyl ether;

Reference yield:

N-[5-Ethyl-3-[2'-(1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-[1,3,4]thiadiazol-(2Z)-ylidene]-2,2,2-trifluoro-acetamide → 5-ethyl-2-imino-3-[2'-(1H-tetrazol-5-yl)-biphenyl-4-yl]methyl-1,3,4-thiadiazoline (167005-94-9)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water; Yield given; Heating;

DOI:10.1016/S0960-894X(96)00250-8

upstream raw materials:

2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

5-ethyl-2-imino-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

butan-1-ol

4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

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