2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

Base Information

Chemical Name:2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline
CAS No.:169328-26-1
Molecular Formula:C₂₀H₁₅F₃N₄OS
Molecular Weight:416.427
Hs Code.:

Synonyms:2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

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Technology Process of 2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

There total 3 articles about 2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 22926-50-7
5-ethyl-2-trifluoroacetylamino-1,3,4-thiadiazole

: 114772-54-2
4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

: 169328-26-1
2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(96)00250-8

Reference yield:

: 22926-50-7
5-ethyl-2-trifluoroacetylamino-1,3,4-thiadiazole

: 7440-44-0
pyrographite

: 114772-54-2
4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

: 169328-26-1
2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

Guidance literature:: With potassium iodide; potassium carbonate; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 114772-53-1
2-Cyano-4'-methylbiphenyl

: 169328-26-1
2-trifluoroacetylimino-5-ethyl-3-(2'-cyanobiphenyl-4-yl)methyl-1,3,4-thiadiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / tetrachloromethane

2: potassium iodide; potassium carbonate / ethanol; water; ethyl acetate; N,N-dimethyl-formamide

With N-Bromosuccinimide; potassium iodide; potassium carbonate; In tetrachloromethane; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;