Technology Process of C24H29NO13
There total 5 articles about C24H29NO13 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; silica gel;
In
chloroform; isopropyl alcohol;
at 0 ℃;
for 2h;
Inert atmosphere;
DOI:10.1039/c2cc17458h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: silver(l) oxide / acetonitrile / 20 °C / Inert atmosphere
2: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol / 2 h / 0 °C / Inert atmosphere
With
sodium tetrahydroborate; silica gel; silver(l) oxide;
In
chloroform; isopropyl alcohol; acetonitrile;
DOI:10.1039/c2cc17458h
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetonitrile / 72 h / 60 °C / Inert atmosphere
2: 17 h / 160 - 165 °C / Inert atmosphere
3: silver(l) oxide / acetonitrile / 20 °C / Inert atmosphere
4: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol / 2 h / 0 °C / Inert atmosphere
With
sodium tetrahydroborate; silica gel; potassium carbonate; silver(l) oxide;
In
chloroform; isopropyl alcohol; acetonitrile;
2: Claisen rearrangement;
DOI:10.1039/c2cc17458h