Technology Process of C28H40O
There total 10 articles about C28H40O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
benzyl bromide;
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 0.166667h;
Inert atmosphere;
C21H34O;
With
tetrabutylammomium bromide;
In
tetrahydrofuran;
at 0 - 35 ℃;
Inert atmosphere;
DOI:10.1016/j.tet.2011.05.092
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.42 h / -60 °C / Inert atmosphere
1.2: 0.17 h / -60 °C / Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C
3.1: pyrrolidine / diethyl ether / 20 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / 0 °C / Inert atmosphere
4.2: 8 h / 0 - 20 °C / Inert atmosphere
5.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere
5.2: 0 - 35 °C / Inert atmosphere
With
pyrrolidine; n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane;
1.1: Swern oxidation / 1.2: Swern oxidation / 4.2: Wittig reaction;
DOI:10.1016/j.tet.2011.05.092