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C28H40O

Base Information
  • Chemical Name:C28H40O
  • CAS No.:1186505-18-9
  • Molecular Formula:C28H40O
  • Molecular Weight:392.625
  • Hs Code.:
C<sub>28</sub>H<sub>40</sub>O

Synonyms:C28H40O

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Chemical Property of C28H40O
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Technology Process of C28H40O

There total 10 articles about C28H40O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
benzyl bromide; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.166667h; Inert atmosphere;
C21H34O; With tetrabutylammomium bromide; In tetrahydrofuran; at 0 - 35 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.05.092
Guidance literature:
With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2009.06.064
Guidance literature:
Multi-step reaction with 5 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.42 h / -60 °C / Inert atmosphere
1.2: 0.17 h / -60 °C / Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C
3.1: pyrrolidine / diethyl ether / 20 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / 0 °C / Inert atmosphere
4.2: 8 h / 0 - 20 °C / Inert atmosphere
5.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere
5.2: 0 - 35 °C / Inert atmosphere
With pyrrolidine; n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 1.1: Swern oxidation / 1.2: Swern oxidation / 4.2: Wittig reaction;
DOI:10.1016/j.tet.2011.05.092
upstream raw materials:

C21H32O

benzyl bromide

C21H34O

C21H34O

Downstream raw materials:

C34H46O5

C34H46O5

C32H42O3

C32H42O3

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