di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane

Base Information

Chemical Name:di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane
CAS No.:1146956-34-4
Molecular Formula:C₂₁H₃₉FOSi₂
Molecular Weight:382.709
Hs Code.:

Synonyms:di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane

Chemical Property:

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Technology Process of di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane

There total 4 articles about di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 558-63-4
di-tert-butyldifluorosilane

: 87736-74-1
4-(tert-butyldimethylsiloxymethyl)bromobenzene

: 1146956-34-4
di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane

Guidance literature:: 4-(tert-butyldimethylsiloxymethyl)bromobenzene; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.5h; Inert atmosphere;

di-tert-butyldifluorosilane; In tetrahydrofuran; pentane; at 20 ℃; for 12h; Inert atmosphere;

Reference yield:

: 873-75-6
4-bromobenzenemethanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1146956-34-4
di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C

2.1: tert.-butyl lithium / pentane; tetrahydrofuran / 0.5 h / -78 °C

2.2: 18 h / -78 - 20 °C

With 1H-imidazole; tert.-butyl lithium; In tetrahydrofuran; N,N-dimethyl-formamide; pentane;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1146956-34-4
di-tert-butyl(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)fluorosilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C / Cooling with ice; Inert atmosphere

2.1: tert.-butyl lithium / pentane; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

2.2: 48 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; tert.-butyl lithium; In diethyl ether; N,N-dimethyl-formamide; pentane;
DOI:10.3390/ph14060547