C₁₆H₁₂BIN₂O

Base Information

Chemical Name:C₁₆H₁₂BIN₂O
CAS No.:1447963-01-0
Molecular Formula:C₁₆H₁₂BIN₂O
Molecular Weight:386
Hs Code.:

C<sub>16</sub>H<sub>12</sub>BIN<sub>2</sub>O

Synonyms:C₁₆H₁₂BIN₂O

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Chemical Property of C₁₆H₁₂BIN₂O

Chemical Property:

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Technology Process of C₁₆H₁₂BIN₂O

There total 3 articles about C₁₆H₁₂BIN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1447963-00-9
2-iodo-5-hydroxyphenylboronic acid

: 479-27-6
naphthalene-1,8-diamine

: 1447963-01-0
C₁₆H₁₂BIN₂O

Guidance literature:: In dimethyl sulfoxide; toluene; at 120 ℃; for 12h; Inert atmosphere; Dean-Stark;
DOI:10.1016/j.tetlet.2013.06.043

Reference yield:

: 89694-50-8
(2-iodo-5-methoxyphenyl)boronic acid

: 1447963-01-0
C₁₆H₁₂BIN₂O

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane; n-heptane / 12 h / -78 - 20 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: toluene; dimethyl sulfoxide / 12 h / 120 °C / Inert atmosphere; Dean-Stark

With boron tribromide; In n-heptane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1016/j.tetlet.2013.06.043

Reference yield:

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 1447963-01-0
C₁₆H₁₂BIN₂O

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; silver nitrate

2.1: boron tribromide / dichloromethane; n-heptane / 12 h / -78 - 20 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

3.1: toluene; dimethyl sulfoxide / 12 h / 120 °C / Inert atmosphere; Dean-Stark

With iodine; boron tribromide; silver nitrate; In n-heptane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1016/j.tetlet.2013.06.043