1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline

Base Information

• Chemical Name: 1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline
• CAS No.: 1629768-58-6
• Molecular Formula: C₂₄H₁₄F₅N₅
• Molecular Weight: 467.401
• Mol file: 1629768-58-6.mol

Synonyms:1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline

Chemical Property of 1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline

There total 1 articles about 1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

perfluorobenzaldehyde (653-37-2) + N-benzyl-N-picolyldiaminomaleonitrile → 1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline (1629768-58-6)

Guidance literature:

With acetic acid; at 20 ℃; for 48h; Inert atmosphere; Schlenk technique; Darkness;

DOI:10.1002/ejic.201402040

Reference yield: 27.0%

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + 1-benzyl-4,5-dicyano-3-picolyl-2-(pentafluorophenyl)imidazoline (1629768-58-6) → [PdCl2{1-benzyl-4,5-dicyano-3-picolylimidazol-2-ylidene}]

Guidance literature:

In chlorobenzene; at 135 ℃; for 2.41667h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1002/ejic.201402040

upstream raw materials:

perfluorobenzaldehyde